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Beilstein J. Org. Chem. 2013, 9, 1083–1092, doi:10.3762/bjoc.9.120
Graphical Abstract
Figure 1: O-Ethoxycarbonyl oximes prepared.
Scheme 1: Photochemical reactions of biphenyl oxime carbonates.
Figure 2: EPR spectrum during photolysis of 1f in t-BuPh at 240 K. Top (black): experimental spectrum. Bottom...
Figure 3: EPR spectrum during photolysis of 2a in t-BuPh at 230 K. Top (blue): experiment; bottom (red): simu...
Scheme 2: Ring closure of iminyl radicals derived from 2a,b.
Figure 4: DFT computed structures for 5a, 11a and their cyclisation transition states (TS). Top line: spin de...